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Photochemistry of Fe(III) hydroxocomplexes has a great interest because of possibility of hydroxylradical formation at the primary photochemical step. This mechanism is based mainly on the analysisof the final products of photochemical reactions between light-excited Fe(III) complexes and organic compounds.However, realization of an alternative mechanism of photolysis, based on the intermolecular electrontransfer from organic molecules located in the second coordination sphere to the light-excited complex couldtake place. To distinguish these mechanisms, the experiments on the nanosecond laser flash photolysis ofFe(OH)aq2+ in water solutions (pH 3) with organic additives; namely nitrobenzene, N,N-dimethylformamide,and phenol have been performed. And the formation of the organic radicals Ph(•OH)NO2, HCON(CH2•)(CH3), and Ph(OH)2•, was observed, respectively. The rate constants of the formation and decay of the radicals coincidewith those found in literature. The results support the formation of the hydroxyl radical upon thephotolysis of Fe(OH)aq2+

international journal of photoenergy

Photodegradation of organic pollutants in aqueous solutions caused by <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" alttext="${\text{Fe}}\left( {{\text{OH}}} \right)_{{\text{aq}}}^{2 + } $" id="E1"><mml:mrow><mml:mtext>Fe</mml:mtext><mml:msub><mml:mrow><mml:mrow><mml:mo>(</mml:mo><mml:mrow><mml:mtext>OH</mml:mtext></mml:mrow><mml:mo>)</mml:mo></mml:mrow></mml:mrow><mml:mrow><mml:mtext>aq</mml:mtext></mml:mrow></mml:msub><mml:mrow><mml:mn>2</mml:mn><mml:mo>+</mml:mo></mml:mrow></mml:…

Photodegradation of organic pollutants in aqueous solutions caused by Fe(OH)aq2+