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Nanocrystalline TiO2 catalysts based on pure rutile (R100) anda 30% of anatase and 70% of rutile (R70) were synthesized by thesol-gel method, using Pluronic PE 6400 as templating agent.Catalysts were characterized in terms of structural andmorphological properties; moreover, the formation of paramagneticcharge carriers under UV irradiation was studied and related tothe activity of TiO2 in the photoinduced degradation of phenol.With respect to Degussa P25, the two sol-gel catalysts show lowersurface area and a wider pore size distribution. The EPR spectrarecorded under UV irradiation show enhanced charge separation inthe sol-gel samples, with the O− species in higher amount thanin Degussa P25. This result is in agreement with the highcatalytic activity of R100 sample in the photoinduced degradationof phenol, very similar to that displayed by Degussa P25 andhigher than that of R70 sample

Nanocrystalline TiO2with enhanced photoinduced charge separation as catalyst for the phenol degradation