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This work investigated the morphological, structural, and vibrational properties of graphite nanoplatelets (GNPs) that were produced by ultrasonication. Scanning and transmission electron microscopy, X-ray diffractometry, and Raman spectroscopy identified 120-nm-thick GNP crystallites and 50–2000 μm2 plates with different areas and shapes. Extensive exfoliation was observed by transmission electron microscopy with abundant multi and some monolayer GNPs. X-ray diffractometry confirmed 43 GNP layers along the  c -axis. Rietveld X-ray analysis indicated a GNP crystal lattice with stacks of parallel two-dimensional graphene layers and tightly bound hybridized carbon atoms stacked in a translational …ABAB… sequence in hexagonal rings. Raman scattering indicated well-defined GNPs with few defects and no oxide content. All analytical results reveal that GNPs could have significant potential application in electrically conductive reinforcement devices.

Investigation of the Morphological, Structural, and Vibrational Behaviour of Graphite Nanoplatelets