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The aim of this investigation was to develop an efficient, rapid, and selective method for the synthesis of ω-alkylenediphosphoric acids (HO)2(O)P-O-CH2n-O-P(O)(OH)2 from reaction of several diols with phosphorus oxychloride. The reaction was investigated using three methodologies: (i) presence of a base, (ii) classical heating, and (iii) use of microwave irradiation. Influence of reaction temperature and molar ratio of reagents, as well as the nature of the solvent, was studied using these three different methods

journal of chemistry

Rapid and Efficient Synthesis of<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" id="M1"><mml:mrow><mml:mi mathvariant="bold-italic">ω</mml:mi></mml:mrow></mml:math>-Alkylenediphosphoric Acids from Phosphorus Oxychloride

Rapid and Efficient Synthesis ofω-Alkylenediphosphoric Acids from Phosphorus Oxychloride