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Novel BiOBr hierarchical microspheres have been successfully prepared via a facile microwave-assisted solvothermal route and used for visible-light photocatalytic degradation of RhB. The phase and morphology of the products were characterized by powder X-ray diffraction (XRD), thermogravimetric analysis (TG), scanning electron microscopy (SEM), BET, and UV-vis diffuse reflectance spectra. The SEM observations displayed that BiOBr flower-like nanostructure assembled from nanosheets. The BiOBr flower-like nanostructure, with a narrow band gap (2.63 eV), shows  excellent photocatalytic activity in the degradation of RhB dye under visible-light, much higher than those of  BiOBr nanosheet and  P25 photocatalysts

Microwave-Solvothermal Synthesis of Nanostructured BiOBr with Excellent Visible-Light Photocatalytic Properties