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Well-dispersed mesoporous γ-alumina microfibers with high surface were prepared by thermal decomposition of the ammonium aluminum carbonate hydroxide (AACH) precursors. The as-synthesized alumina retained the morphology of its precursor and exhibited memory effect. The structural, morphological, porous, and adsorptive properties of the samples were investigated by XRD, FTIR, TGA-DSC, SEM, TEM, and UV-vis spectroscopy. The prepared γ-alumina microfibers exhibited excellent ability to remove organic pollutants from waste water because of their mesoporous structures. The γ-alumina in situ converted from AACH synthesized without surfactant exhibited adsorption ability for Congo red as good as that synthesized with PEG2000 and better than PEG20000 that provided a facile method without surfactant to synthesize γ-alumina with excellent adsorption performance.

Mesoporous Alumina Microfibers In Situ Transformation from AACH Fibers and the Adsorption Performance