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Well-defined nanosheet-assembled (BiOCl)x(ZnO)1−x nanoflowers were synthesized by a solvothermal method. It was found that ZnO nanoparticles were anchored on the flower-like BiOCl nanostructures, as demonstrated by varying the initial compositions of the Bi precursor and the volume ratios of mixed solvents (ethylene glycol to water). The as-prepared (BiOCl)0.6(ZnO)0.4 nanocomposites showed enhanced photocatalytic activity toward rhodamine B degradation under ultraviolet (UV) irradiation. And the photocatalytic mechanism was discussed in detail.

Facile Solvothermal Synthesis of BiOCl/ZnO Heterostructures with Enhanced Photocatalytic Activity