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N-Heterocyclic carbenes catalyzed hydrophosphonylation reaction of   α  -ketoesters and   α  -trifluoromethyl ketones was developed. Under the catalysis of 10 mol% IPr,   α  -ketoesters or   α  -trifluoromethyl ketones reacted with dialkyl phosphites to provide quaternary   α  -hydroxyphosphonates in good to excellent yield.

the scientific world journal/thescientificworldjournal

NHCs Catalyzed Hydrophosphonylation of<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" id="M1"><mml:mrow><mml:mi mathvariant="bold-italic">α</mml:mi></mml:mrow></mml:math>-Ketoesters and<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" id="M2"><mml:mrow><mml:mi mathvariant="bold-italic">α</mml:mi></mml:mrow></mml:math>-Trifluoromethyl Ketones

NHCs Catalyzed Hydrophosphonylation ofα-Ketoesters andα-Trifluoromethyl Ketones