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Six specimens of an aluminum alloy (AA-5083) extruded by Equal Channel Angular Pressing following two different routes plus a blank sample were examined with a neutron radiation of 1.5448 Å. Macrostrain maps from the (311) reflection were obtained. A clear difference about accumulated macrostrain with the extrusion cycles between the two routes is shown. The diffraction data of annealed specimens did permit to estimate crystallite sizes that range between 89 nm and 115 nm depending on the routes

journal of nanomaterials

Strain Mapping and Nanocrystallite Size Determination by Neutron Diffraction in an Aluminum Alloy (AA5083) Severely Plastically Deformed through Equal Channel Angular Pressing