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GdF3:Eu3+ nanophosphors with hexagonal or orthorhombic structure have been succeeded to be selectively synthesized at room temperature for the first time via a simple soft chemical route. The structure and morphology of GdF3:Eu3+ nanophosphors were controlled by using different fluoride precursors. Hexagonal GdF3:Eu3+ nanocrystals were formed when NaBF4 was used as a fluoride precursor, while orthorhombic GdF3:Eu3+ nanocrystals were obtained with NaF or NH4F fluoride precursor. It was also experimentally revealed that hexagonal GdF3:Eu3+ nanophosphors emitted essentially stronger Eu3+ luminescence than orthorhombic ones did. The formation mechanism of GdF3 nanocrystals and the possible reasons of the strong PL in hexagonal were discussed

Selective Synthesis and Luminescence Properties of Nanocrystalline GdF3:Eu3+with Hexagonal and Orthorhombic Structures

Selective Synthesis and Luminescence Properties of Nanocrystalline GdF3:Eu³⁺with Hexagonal and Orthorhombic Structures