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Secondary lithium sulfur (Li-S) batteries have been heavily studied in the battery community since the start of the 21 century due to their high theoretical capacity and specific energy density. The ground-breaking lithium ion battery has revolutionized society and its ability to store energy, however the lithium ion battery is reaching its limit with a theoretical capacity almost five times lower than that of lithium sulfur. With the improvement and commercialization of Li-S batteries, electric vehicles and personal electronics will have extended performance on a single charge. The viability of this promising chemistry relies on overcoming several key difficulties, one of the most imperative being high solubility, mobility, and reactivity of polysulfide reaction intermediates in liquid electrolytes. In situ Raman microscopy is used to study polysulfide speciation in the bulk electrolyte (1:1 1,2-dimethoxyethane (DME): 1,3-dioxolane (DOL) with 1 M lithium bis(trifluoromethane)sulfonimide (LiTFSI) and 0.25 M LiNO3) during

Study of Polysulfide Speciation in Lithium Sulfur Batteries Using in Situ Confocal Raman Microscopy