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The oxygen reduction reaction (ORR) activity of Pt and Pt3Co nanoparticles deposited on high surface area carbon (Vulcan XC72) was correlated to the ir structural, morphological and compositional changes prior/after accelerated electrochemical ageing tests. These tests consisted of stepping the potential during 1 min successively between potentials of 0.9 and 0.1 V vs. RHE or between 0.9 and 0.6 V vs. RHE for 15 h in Nafion ®

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Identical Location Transmission Electron Microscopy in Polymer Electrolyte Environment – Application to the Degradation of Pt/C and Pt3co/C Electrocatalysts Under Accelerated Aging Tests