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The synthesis process of cobalt nanoparticles via electroless deposition in ethylene glycol (EG) was investigated by electrochemical quartz crystal microbalance (QCM). The oxidation–reduction potential of the Co(II)/Co redox pair in EG could not be thermodynamically calculated because of insufficient thermodynamic data in organic solvents. We experimentally determined the oxidation–reduction potential of the Co(II)/Co redox pair in EG by cyclic voltammetry combined with QCM. The reaction start and end points were also determined by QCM. The effect of the nucleating agent H2PtCl6·6H2O on the cobalt deposition behavior and particle size distribution was examined

Electrochemical QCM Study of the Synthesis Process of Cobalt Nanoparticles via Electroless Deposition