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An electrochemical study of iron was carried out in KCl+LiCl+NaCl melt at 550C using a glassy carbon working electrode. Cyclic voltammetry showed that the Fe(II)/Fe(0) electron exchange is a soluble/insoluble reversible process. The diffusion coefficient of Fe(II) was calculated using cyclic voltammetry; 1.4×10-5 cm2 s-1. For the Fe(II)/Fe(III) red/ox reaction, analysis of the voltammograms suggests that the process is not reversible and is coupled with a chemical reaction. The stability of FeCl 3 and the effect of equilibrium between FeCl 3 and FeCl 2 are also briefly discussed.

Electrochemical Behaviour of Dissolved Iron Chloride in KCl+LiCl+NaCl Melt at 550ºC