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Electrolysis has been performed on a fused mixture of magnesium chloride,potassium chloride, and magnesium borate at 600 oC under an Ar atmosphere usinga graphite anode and a Pt cathode. Magnetic measurements and X-raydiffractometry have revealed that the resultant deposit on the cathode containsa few tens molar percent of MgB2. A voltanmetric measurement at the initialstage of electrolysis has shown that the threshold cathode voltage for theformation of MgB2 from the molten salts is -1.6 V.

Electrochemical Synthesis of Superconductive Boride MgB2 from Molten Salts