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Selenium (Se) is an element monitored by water quality agencies worldwide. The challenge of assessing its presence in aquatic systems is its low concentrations (parts per trillion) and the need for determining its chemical speciation. A method was developed using an ion chromatograph (IC) paired with a quadrupole inductively coupled plasma mass spectrometer (ICP-MS) equipped with a hydrogen reaction cell to provide analysts with a rapid and sensitive method to measure Se speciation with suitable accuracy and precision. The Se species selenite (SeIV) and selenate (SeVI) were separated within a 5 min span using dilute nitric acid as a mobile phase in a step-wise gradient (50–400 mmol L−1) and quantified using 80Se isotope that yielded low limits of detection (<10 ng L−1). Spectral interference from plasma generated diatomic argon ions (40Ar2+; m/z = 80) on 80Se was eliminated by hydrogen gas (H2) in the reaction cell. Polyatomic 79Br1H+ (m/z = 80) did not interfere with 80Se for quantification of common aqu...

A rapid and sensitive IC-ICP-MS method for determining selenium speciation in natural waters