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A novel method for incorporation of palladium nanoparticles into a poroushypercrosslinked polystyrene matrix has been developed. The composite obtainedby reduction of [Pd(π-allyl)Cl] 2  with hydrogen insupercritical CO 2  shows high catalytic activity in thehydrogenation of benzene and can be used twelve (12) times in a row without anydecrease in conversion rate. The catalyst is also suitable for quantitativehydrogenation of toluene, tetralin and phenol. The obtained catalytic system iscompared with the palladium composite synthesized by a conventional method basedon hypercrosslinked polystyrene.

Palladium Nanoparticles in Hypercrosslinked Polystyrene: Synthesis and Application in the Hydrogenation of Arenes