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Using synchrotron radiation with a photon energy of 15 keV, the molecularstructure of an adsorbed n-triacontanol layer at the n-hexadecane - waterinterface in different its phase states has been studied by the method ofdiffuse X-ray scattering. The analysis of the experimental data shows that atransition to the multilayer adsorption occurs at a temperature below thetwo-dimensional vapor - liquid transition at the interface. This transition hasbeen attributed to a feature in the temperature dependence of the concentrationof micelles in a surface layer 100 - 200 {\AA} thick.

X-Ray Study of Thermotropic Mesophases of an n-Triacontanol Adsorption Film at the n-Hexadecane - Water Interface