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Fe2O3 nanodeposits have been grown on fluorine-doped tin oxide (FTO) substrates by plasma\udenhanced-chemical vapor deposition (PE-CVD). Subsequently, the obtained systems have been\udfunctionalized through the sequential introduction of TiO2 and Au nanoparticles (NPs) by means of\udradio frequency (RF)-sputtering. The target nanocomposites have been specifically optimized in\udview of their ultimate functional application in solar-driven H2 generation. In the present study, our\udattention is focused on a detailed X-ray photoelectron spectroscopy (XPS) characterization of the\udsurface composition for a representative Fe2O3-TiO2-Au specimen. In particular, this report\udprovides a detailed discussion of the analyzed C 1s, O 1s, Fe 2p, Ti 2p, and Au 4f regions. The\udobtained results point to the formation of pure Fe2O3-TiO2-Au composites, with gold present only\udin its metallic state and each of the constituents maintaining its chemical identity

XPS analysis of Fe2O3-TiO2-Au nanocomposites prepared by a plasma-assisted route