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An (Al,Cu) 13 (Fe,Cu) 4 phase of [trideca(aluminium/copper) tetra(iron/copper)] was obtained by the high-pressure sintering (HPS) process of a mixture with composition Al 78 Cu 15 Fe 7 . Structure analysis suggests that Cu atoms can replace both Al and Fe atoms. Such findings support previous anomalous X-ray scattering (AXS) results although deviate from other reports. The new phase adopts the λ-Al 13 Fe 4 structure type where Cu atoms partially occupy the 2 c and 4 i sites for Al and Fe atoms, respectively, with occupancies of 0.233 (5) and 0.173 (16).

Crystal structure of the λ-Al13Fe4-type intermetallic (Al,Cu)13(Fe,Cu)4

Crystal structure of the λ-Al₁₃Fe₄-type intermetallic (Al,Cu)₁₃(Fe,Cu)₄