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Crystals of the phase Al 10 Ni 3 Fe 0.83 (decaaluminium trinickel iron) were obtained by high-pressure sintering (HPS) of a stoichiometric mixture with nominal composition Al 71 Ni 24 Fe 5 . Al 10 Ni 3 Fe 0.83 adopts the Co 2 Al 5 structure type in the space group type P 6 3 / mmc with the unique Fe site on site 2 c partially occupied (occupancy 0.83).

Al10Ni3Fe0.83, an Fe-depleted phase in the Al–Ni–Fe system

Al₁₀Ni₃Fe_0.83, an Fe-depleted phase in the Al–Ni–Fe system