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The formation and crystal structure of a zigzag molecular network held together by I...N halogen bonds is reported. In particular, the halogen-bond donor is 1,2-diiodoperchlorobenzene ( 1,2-C 6 I 2 Cl 4 ) while the acceptor is a head-to-tail photoproduct, namely  rctt -1,3-bis(pyridin-4-yl)-2,4-diphenylcyclobutane ( ht -PP ). In this co-crystal ( 1,2-C 6 I 2 Cl 4 )·( ht -PP ), the donor acts as a bent two-connected node while the acceptor behaves as a linear linker to form the extended solid. Neighbouring chains pack in a tongue-and-groove-like pattern that engage in various Cl...π interactions to both the phenyl and pyridyl rings resulting in a supramolecular two-dimensional sheet.

acta crystallographica. section e, crystallographic communications

Halogen-bonded zigzag molecular network based upon 1,2-diiodoperchlorobenzene and the photoproduct <i>rctt</i>-1,3-bis(pyridin-4-yl)-2,4-diphenylcyclobutane

Halogen-bonded zigzag molecular network based upon 1,2-diiodoperchlorobenzene and the photoproduct rctt-1,3-bis(pyridin-4-yl)-2,4-diphenylcyclobutane