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Studies of the coordination chemistry between the di-phenyl-amide ligand, NPh 2 , and the smaller rare-earth Ln  III ions, Ln = Y, Dy, and Er, led to the structural characterization by single-crystal X-ray diffraction crystallography of both solvated and unsolvated complexes, namely, tris-(di-phenyl-amido-κ N )bis-(tetrahydro-furan-κ O )yttrium(III), Y(NPh 2 ) 3 (THF) 2 or [Y(C 12 H 10 N) 3 (C 4 H 8 O) 2 ], 1-Y , and the erbium(III) (Er), 1-Er , analogue, and bis-[μ-1κ N :2(η 6 )-di-phenyl-amido]-bis-[bis-(di-phenyl-amido-κ N )yttrium(III)], [(Ph 2 N) 2 Y(μ-NPh 2 )] 2 or [Y 2 (C 12 H 10 N) 6 ], 2-Y , and the dysprosium(III) (Dy), 2-Dy , analogue. The THF ligands of 1-Er are modeled with disorder across two positions with occupancies of 0.627 (12):0.323 (12) and 0.633 (7):0.367 (7). Also structurally characterized was the tetra-metallic Er III bridging oxide hydrolysis product, bis-(μ-di-phenyl-amido-κ 2  N : N )bis-[μ-1κ N :2(η 6 )-di-phenyl-amido]-tetra-kis-(di-phenyl-amido-κ N )di-μ 3 -oxido-tetra-erbium(III) benzene disolvate, {[(Ph 2 N)Er(μ-NPh 2 )] 4 (μ-O) 2 }·(C 6 H 6 ) 2 or [Er 4 (C 12 H 10 N) 8 O 2 ]·2C 6 H 6 , 3-Er . The 3-Er structure was refined as a three-component twin with occupancies 0.7375:0.2010:0.0615.

acta crystallographica. section e, crystallographic communications

Synthesis and crystallographic characterization of diphenylamide rare-earth metal complexes Ln(NPh2)3(THF)2 and [(Ph2N)2 Ln(μ-NPh2)]2