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Single crystals of strontium tetra-cobalt tris-(orthophosphate) hydroxide, SrCo 4 (OH)(PO 4 ) 3 , were grown serendipitously under hydro-thermal conditions at 473 K. The crystal structure consists of undulating chains of edge-sharing [CoO 6 ] octa-hedra that are linked into (010) layers by common vertices between chains. Adjacent layers are linked along [010] into a framework structure by tetra-hedral [CoO 4 ] units and by PO 4 tetra-hedra. The framework delimits channels extending along [100] in which the eleven-coordinate strontium cations are situated. Bifurcated O-H⋯O hydrogen bonds of weak strengths consolidate the crystal packing. The title compound was also characterized by infrared spectroscopy.

Crystal structure of SrCo4(OH)(PO4)3, a new hydroxyphosphate