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The heterobifunctional organic ligand, 3-(1,2,4-triazol-4-yl)adamantane-1-carboxyl-ate ( tr-ad-COO -  ), was employed for the synthesis of the title silver(I) coordination polymer, {[Ag(C 13 H 16 N 3 O 2 )]·2H 2 O}  n  , crystallizing in the rare ortho-rhom-bic C 222 1 space group. Alternation of the double μ 2 -1,2,4-triazole and μ 2 -η 2 :η 1 -COO - (chelating, bridging mode) bridges between Ag I cations supports the formation of sinusoidal coordination chains. The Ag I centers possess a distorted {N 2 O 3 } square-pyramidal arrangement with τ 5 = 0.30. The angular organic linkers connect the chains into a tetra-gonal framework with small channels along the c- axis direction occupied by water mol-ecules of crystallization, which are inter-linked via O-H⋯O hydrogen bonds with carboxyl-ate groups, leading to right- and left-handed helical dispositions.

acta crystallographica. section e, crystallographic communications

Crystal structure of poly[[[μ4-3-(1,2,4-triazol-4-yl)adamantane-1-carboxylato-κ5 N 1:N 2:O 1:O 1,O 1′]silver(I)] dihydrate]