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The crystal structures of dirubidium potassium dysprosium bis-(vanadate), Rb 2 KDy(VO 4 ) 2 , and caesium potassium gadolinium bis-(vanadate), Cs 1.52 K 1.48 Gd(VO 4 ) 2 , were solved from single-crystal X-ray diffraction data. Both compounds, synthesized by the reactive flux method, crystallize in the space group P  m 1 with the glaserite structure type. VO 4 tetra-hedra are linked to DyO 6 or GdO 6 octa-hedra by common vertices to form sheets stacking along the c axis. The large twelve-coordinate Cs + or Rb + cations are sandwiched between these layers in tunnels along the a and b axes, while the K + cations, surrounded by ten oxygen atoms, are localized in cavities.

acta crystallographica. section e, crystallographic communications

Two new glaserite-type orthovanadates: Rb2KDy(VO4)2 and Cs1.52K1.48Gd(VO4)2