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The crystal structure of the title mol-ecular complex, [Ag 2 {VO 2 F 2 } 2 (C 13 H 17 N 3 O 2 ) 4 ]·4H 2 O, supported by the heterofunctional ligand tr-ad-COOH [1-(1,2,4-triazol-4-yl)-3-carb-oxy-adamantane] is reported. Four 1,2,4-triazole groups of the ligand link two Ag I atoms, as well as Ag I and V V centres, forming the heterobimetallic coordination cluster {Ag I  2 (V V O 2 F 2 ) 2 ( tr ) 4 }. V V exists as a vanadium oxofluoride anion and possesses a distorted trigonal-bipyramidal coordination environment [VO 2 F 2 N]. A carb-oxy-lic acid functional group of the ligand stays in a neutral form and is involved in hydrogen bonding with solvent water mol-ecules and VO 2 F 2  - ions of adjacent mol-ecules. The extended hydrogen-bonding network is responsible for the crystal packing in the structure.

acta crystallographica. section e, crystallographic communications

Crystal structure of tetrakis[μ-3-carboxy-1-(1,2,4-triazol-4-yl)adamantane-κ2 N 1:N 2]tetrafluoridodi-μ2-oxido-dioxidodisilver(I)divanadium(V) tetrahydrate