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In the title compound, [(  t  BuSiMe 2 O) 2 MoO 2 (2,2'-bi-pyridine)] or [Mo(C 6 H 15 OSi) 2 O 2 (C 10 H 8 N 2 )], the Mo VI atom has a distorted octa-hedral environment with the sil-oxy substituents occupying the trans positions. The complex contains a rare ( R  3 SiO) 2  M O 2 ( M = Mo, W) structural motif and was formed in a reaction between sodium molybdate and tert -butyl-dimethyl-silyl chloride in the presence of 2,2-bi-pyridine. In the crystal, neighbouring mol-ecules are linked by C-H⋯O=Mo hydrogen bonds, forming chains propagating along the a -axis direction.

acta crystallographica. section e, crystallographic communications

Crystal structure of (2,2′-bipyridine-κ2 N,N′)-trans-bis(tert-butyldimethylsilyloxy)-cis-dioxidomolybdenum(VI)