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The title lanthanide complexes, [ Ln (DAPBH 2 )(CH 3 OH)(H 2 O) 3 ]Cl 3 ·2CH 3 OH [ Ln  III = Tb and Dy; DAPBH 2 = 2,6-di-acetyl-pyridine bis-(benzoyl-hydrazone), C 23 H 21 N 5 O 2 ], are isotypic. The central lanthanide ions are nine-coordinate, being ligated by three N and two O atoms from the penta-dentate DAPBH 2 ligand, and four O atoms from the coordinated methanol mol-ecule and three coordinated water mol-ecules. The coordination geometry of the lanthanide ion is a distorted capped square anti-prism. In the crystals, the various components are linked by O-H⋯Cl, N-H⋯Cl and O-H⋯O hydrogen bonds, forming three-dimensional supra-molecular frameworks. Within the frameworks, there are C-H⋯Cl and C-H⋯O hydrogen bonds and offset π-π inter-actions (inter-centroid distance ca 3.81 Å).

acta crystallographica. section e, crystallographic communications

Crystal structures of two isotypic lanthanide(III) complexes: triaqua[2,6-diacetylpyridine bis(benzoylhydrazone)]methanollanthanide(III) trichloride methanol disolvates (<i>Ln</i> <sup>III</sup> = Tb and Dy)

Crystal structures of two isotypic lanthanide(III) complexes: triaqua[2,6-diacetylpyridine bis(benzoylhydrazone)]methanollanthanide(III) trichloride methanol disolvates (Ln III = Tb and Dy)

Crystal structures of two isotypic lanthanide(III) complexes: triaqua[2,6-diacetylpyridine bis(benzoylhydrazone)]methanollanthanide(III) trichloride methanol disolvates (Ln ^III = Tb and Dy)