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There are few reports that describe crystal structures of compounds containing cobalt complexed to either dimethyl sulfoxide (Me 2 SO) or quinoline (C 9 H 7 N). The title compound, [Co(C 2 H 6 OS) 6 ][CoCl 3 (C 9 H 7 N)] 2 , is a cobalt salt in which the metal ion is complexed to both Me 2 SO and quinoline. In particular, we observed that anhydrous cobalt(II) chloride reacts with quinoline in Me 2 SO to form a salt that is to be formulated as [Co II (Me 2 SO) 6 ] 2+ {[Co II Cl 3 quinoline] 2  - }. The Co II atom in the cation portion of this mol-ecule lies on a inversion center and is bound to the O atoms of six Me 2 SO moieties in an octa-hedral configuration, while the Co II atom in the anion is attached to three chloride ligands and one quinoline moiety in a tetra-hedral arrangement.

Crystal structure of hexakis(dimethyl sulfoxide-κO)cobalt(II) bis[trichlorido(quinoline-κN)cobaltate(II)]