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The synthesis and the crystal structure of a new halide-bridged polymer, namely catena -poly[bis-(1,2,3-benzotriazolium) [[tetra-chlorido-bis-muth(III)]-μ-chlorido] dihydrate], {(C 6 H 6 N 3 ) 2 [BiCl 5 ]·2H 2 O}  n  are reported. The structure comprises polyanionic zigzag chains of formula [(BiCl 5 ) 2- ]  n  running along the c- axis direction. The 1,2,3-benzotriazolium cations are linked between these polymer chains, via the water mol-ecules, giving rise to left- and right-handed helical chains. Hirshfeld surface analysis and fingerprint plots were used to decode the inter-molecular inter-actions in the crystal network and determine the contribution of the component units for the construction of the three-dimensional architecture.

acta crystallographica. section e, crystallographic communications

Synthesis, crystal structure and Hirshfeld surface analysis of a polymeric bismuthate(III) halide complex, (C6H6N3)2[BiCl5]·2H2O