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The structure of the title compound, C 23 H 26 O 5 or CH 2 =C(CH 3 )-C(O)O-C 6 H 4 -O(O)C-C 6 H 4 -OC 6 H 13 , has been determined. The mol-ecule is non-planar and the dihedral angle between the phenyl rings is 50.72 (4)°. The crystal packing differs from those typical for mesogenic compounds. Only a weak directional inter-action of the C-H⋯O type combines mol-ecules in endless chains running along the a axis.

Crystal structure of 4-[(3-methylbut-3-enoyl)oxy]phenyl 4-n-hexyloxybenzoate