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The hexa-nuclear title compound, [{Cu 3 (μ 3 -OCH 3 )(μ-C 3 H 2 ClN 2 ) 3 } 2 (μ-C 3 H 2 ClN 2 ) 3 (μ 6 -Cl)] or [Cu 6 (C 3 H 2 ClN 2 ) 9 (CH 3 O) 2 Cl], crystallizes in the space group Pbcn , with individual mol-ecules being located on a twofold rotation axis. The mol-ecule adopts a trigonal prismatic shape, with two trinuclear units linked by three 4-chloro-pyrazolate ligand bridges by encapsulating a Cl - anion in a μ 6 -coordination mode. In the crystal, individual mol-ecules are stacked into rods parallel to [1-10] that are arranged in a pseudo-hexa-gonal packing. Cohesion between mol-ecules is accomplished through weak C-H⋯Cl inter-actions.

Crystal structure of μ6-chlorido-nonakis(μ-4-chloropyrazolato)bis-μ3-methoxo-hexacopper(II)

Crystal structure of μ₆-chlorido-nonakis(μ-4-chloropyrazolato)bis-μ₃-methoxo-hexacopper(II)