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The reaction of Cp(CO) 2 FeI with 2-ethynyl-pyridine under Sonogashira conditions [5% PdCl 2 (PPh 3 ) 2 , 10% CuI, THF-NEt 3 (2:1)] afforded the title binuclear μ-pyridyl-vinyl-idene FePd complex ( FePd1 ) as a benzene solvate, [FePd(C 5 H 5 )(C 7 H 5 N)I(CO) 2 ]·C 6 H 6 , in a very low yield rather than the expected iron o -pyridyl-ethynyl complex Cp(CO) 2 Fe-C≡C-(2-C 5 H 4 N). The Fe and Pd atoms in FePd1 are bridged by carbonyl and pyridyl-vinyl-idene ligands, the pyridyl N atom being bonded to the palladium atom. The use of equimolar amounts of PdCl 2 increases the yield of FePd1 to 12%. The reaction pathway leading to FePd1 is proposed.

acta crystallographica. section e, crystallographic communications

Crystal structure of μ-carbonyl-1:2κ2C:C-carbonyl-1κC-(1η5-cyclopentadienyl)iodido-2κI-[μ-2-(pyridin-2-yl)ethene-1,1-diyl-1κC1:2κ2N,C1]ironpalladium(Fe—Pd) benzene monosolvate