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The title compound, [Fe 3 (C 11 H 11 N 2 O 5 ) 2 Cl 3 (C 2 H 6 OS) 3 ] 2 ·7C 2 H 6 OS·2H 2 O, was isolated accidentally from an Fe 0 -NiCl 2 ·6H 2 O-H 3  L -TEA-DMSO system [where H 3  L is the product of the condensation between p -nitro-salicyl-aldehyde and 2-amino-2-methyl-propane-1,3-diol and dimethyl sulfoxide (DMSO), and TEA is triethylamine]. The structure is based on a trinuclear {Fe 3 (μ-O) 4 } core, with an angular arrangement of the Fe III ions that can be explained by the geometrical restrictions of two bulky ligands, each coordinating to all of the metal cations.

acta crystallographica. section e, crystallographic communications

Crystal structure of bis(bis{μ<sub>3</sub>-3-methyl-3-[(4-nitro-2-oxidobenzylidene)amino]propane-1,3-diolato}tris[chlorido(dimethyl sulfoxide)iron(III)]) dimethyl sulfoxide heptasolvate dihydrate

Crystal structure of bis(bis{μ3-3-methyl-3-[(4-nitro-2-oxidobenzylidene)amino]propane-1,3-diolato}tris[chlorido(dimethyl sulfoxide)iron(III)]) dimethyl sulfoxide heptasolvate dihydrate

Crystal structure of bis(bis{μ₃-3-methyl-3-[(4-nitro-2-oxidobenzylidene)amino]propane-1,3-diolato}tris[chlorido(dimethyl sulfoxide)iron(III)]) dimethyl sulfoxide heptasolvate dihydrate