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The title hydrated complex, [Cu 2 (C 7 H 4 O 3 )(C 12 H 8 N 2 ) 4 ](C 7 H 5 O 3 ) 2 ·7.5H 2 O, is composed of dinuclear Cu II complex cations, noncoordinating 4-hy-droxy-benzoate anions and water mol-ecules of crystallization. In the dinuclear complex cation, the Cu II ions are bridged by a 4-oxidobenzoate ligand and thus each metal ion is five-coordinated by two chelating 1,10-phenanthroline (phen) mol-ecules and one anionic O atom in a distorted trigonal-bipyramid geometry. In the crystal, aromatic π-π stacking occurs between phen rings of neighbouring dinuclear Cu II complex cations, forming two-dimensional supra-molecular systems parallel to (100).

acta crystallographica. section e, crystallographic communications

Crystal structure of μ-4-oxidobenzoato-κ2O1:O4-bis[bis(1,10-phenanthroline-κ2N,N′)copper(II)] bis(4-hydroxybenzoate) 7.5-hydrate