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The crystalline sponge method facilitates the X-ray structure determination of samples that do not crystallize or are too sparsely available to afford viable crystallization. By including these materials in a metal–organic framework, the structure of the guest molecules can be determined. Some of the inherent difficulties of this method are discussed and the use of Cu  K β radiation is presented as a simple and effective means to improve the quality of the diffraction data that can be obtained from a sponge crystal.

The benefits of Cu Kβ radiation for the single-crystal X-ray structure determination of crystalline sponges