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The crystal structure of tris­odium potassium dodeca­molybdenum tetra­deca­sulfide, Na 2.9 (2) KMo 12 S 14 , consists of Mo 12 S 14 S 6  cluster units inter­connected through inter­unit Mo—S bonds and delimiting channels in which the Na +  cations are disordered. The cluster units are centered at Wyckoff positions 2 d  and have point-group symmetry 3.2. The K atom lies on sites with 3.2 symmetry (Wyckoff site 2 c ) between two consecutive Mo 12 S 14 S 6  units. One of the three independent S atoms and one Na atom lie on sites with 3.. symmetry (Wyckoff sites 4 e  and 4 f ). The other Na atom occupies a 2 b  position with -3.. symmetry. The crystal studied was a merohedral twin with refined components of 0.4951 (13) and 0.5049 (13).

acta crystallographica. section e

Na2.9KMo12S14: a novel quaternary reduced molybdenum sulfide containing Mo12clusters with a channel structure