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In the title compound, [RhH(C 74 H 68 O 8 P 2 )(C 18 H 15 P)(CO)]·3C 4 H 10 O, the CHP 3  coordination set at the Rh I  ion is arranged in a distorted trigonal–bipyramidal geometry with the P atoms adopting equatorial coordination sites and the C atom of the carbonyl ligand as well as the H atom adopting the axial sites. The asymmetric unit contains two very similar mol­ecules of the rhodium complex, two half-occupied diethyl ether mol­ecules and further diethyl ether solvent mol­ecules which could not be modelled successfully. Therefore contributions of the latter were removed from the diffraction data using the SQUEEZE procedure in  PLATON  [Spek (2009  ▶ ).  Acta Cryst.  D 65 , 148–155].

acta crystallographica. section e

Carbonyl{3,3′-di-tert-butyl-5,5′-dimethoxy-2,2′-bis[(4,4,5,5-tetramethyl-1,3,2-dioxaphospholan-2-yl)oxy]biphenyl-κ2P,P′}hydrido(triphenylphosphane-κP)rhodium(I) diethyl ether trisolvate