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The title compound, [Li 2 Mg(C 4 H 3 F 6 O) 4 (C 4 H 10 O 2 ) 2 ], forms as a white crystalline powder by-product of the reaction of lithium 1,1,1,3,3,3-hexa­fluoro-2-methyl-2-propoxide with Mo(N-2,6-Me 2 —C 6 H 3 )(CHCMe 2 Ph)(O 3 SCF 3 ) 2 ·2DME (DME is 1,2-dimethoxyethane) contaminated with MgCl 2 . The crystal structure of this compound contains half a mol­ecule in the asymmetric unit, with a twofold rotation axis through the central Mg 2+  cation. The four 1,1,1,3,3,3-hexa­fluoro-2-methyl­propan-2-olate ligands serve as bridging ligands connecting the Li +  and Mg 2+  cations. The Li +  cation is additionally stabilized by a DME ligand. This results in a distorted tetra­hedral ligand field around both the Mg 2+  and Li +  cations.

acta crystallographica. section e

Bis(1,2-dimethoxyethane)-1κ2O,O′;3κ2O,O′-tetrakis(μ-1,1,1,3,3,3-hexafluoro-2-methylpropan-2-olato)-1:2κ4O:O;2:3κ4O:O-1,3-dilithium-2-magnesium