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The title structure, [Rh 2 (C 11 H 14 NO) 4 (C 7 H 5 N) 2 ], contains a dinuclear Rh complex of point symmetry -4 with an Rh—Rh unit and two benzonitrile ligands located in special positions along the twofold axis passing through -4. Four symmetry-equivalent mesitylacetamidate ligands bridge the Rh—Rh unit. Thus, each Rh II  atom has an approximately octa­hedral coordination by one Rh [Rh—Rh = 2.4290 (6) Å], two acetamidate O atoms  trans  to each other [Rh—O = 2.044 (3) Å], two acetamidate N atoms  trans  to each other [Rh—N = 2.091 (4) Å], and a benzonitrile N atom  trans  to Rh [Rh—N = 2.222 (3) Å]. The structure is held together by weak van der Waals forces.

acta crystallographica. section e

Tetrakis[μ-N-(2,4,6-trimethylphenyl)acetamidato]-κ4N:O;κ4O:N-bis[(benzonitrile-κN)rhodium(II)](Rh—Rh)