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The reaction of NiCl 2 ·6H 2 O with sodium 2,2-dicyano­ethene-1,1-dithiol­ate [Na 2 ( i -mnt)] in dimethyl sulfoxide produces the title complex, [Ni(C 2 H 6 OS) 6 ][Ni(C 4 N 2 S 2 ) 2 ]. There is half each of an [Ni(C 2 H 6 OS) 6 ] 2−  complex anion and an [Ni{(CH 3 ) 2 SO} 6 ] 2+  complex cation in the asymmetric unit. The  i -mnt ligand coordinates in a bidentate manner to the Ni atom in the anion through the two chelating S atoms in an approximate square-planar geometry. The Ni atom in the complex cation has an octahedral coordination environment with six dimethyl sulfoxide mol­ecules as ligands.

Hexakis(dimethyl sulfoxide-κO)nickel(II) bis(2,2-dicyanoethene-1,1-dithiolato-κ2S,S′)nickelate(II)

Hexakis(dimethyl sulfoxide-κO)nickel(II) bis(2,2-dicyanoethene-1,1-dithiolato-κ²S,S′)nickelate(II)