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In the crystal structure of the title compound, {[Co(NCS) 2 (C 6 H 4 N 2 ) 4 ]·2C 4 H 8 O 2 }, the Co II  cations are octa­hedrally coordinated by two terminal  N -bonded thio­cyanate anions and four  N -bonded 3-cyano­pyridine ligands. The asymmetric unit consists of one Co II  cation, which is located on a special position with site symmetry 2/ m , one thio­cyanate anion and one dioxane mol­ecule, located on a crystallographic mirror plane, as well as one 3-cyano­pyridine ligand in a general position. The crystal structure consists of discrete complexes of [Co(NCS) 2 (3-cyano­pyridine) 4 ], as well as two non-coordinating 1,4-dioxane solvent mol­ecules which are disordered due to symmetry.

Tetrakis(3-cyanopyridine-κN1)bis(thiocyanato-κN)cobalt(II) 1,4-dioxane disolvate

Tetrakis(3-cyanopyridine-κN¹)bis(thiocyanato-κN)cobalt(II) 1,4-dioxane disolvate