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A preliminary X-ray study of CaPtAl has been reported previously by Hulliger [ J. Alloys Compd  (1993),  196 , 225–228] based on X-ray powder diffraction data without structure refinement. With the present single-crystal X-ray study, we confirm the assignment of the TiNiSi type for CaPtAl, in a fully ordered inverse structure. All three atoms of the asymmetric unit have . m . site symmetry. The structure features a  ∞3 [AlPt] open framework with a fourfold coordination of Pt by Al atoms and  vice versa . The Ca atoms are located in the large channels of the structure.

Calcium platinum aluminium, CaPtAl