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In the title co-crystal, C 18 H 12 N 6 O 2 ·CHCl 3 , intra­molecular Cl 3 C—H⋯N hydrogen-bonding inter­actions occur between a single CHCl 3  and both N atoms at the 1,10-positions on the phenanthroline portion of the mol­ecule. The inter­planar distance between inversion-related mol­ecules is 3.241 (2) Å.

10,12-Dimethylpteridino[6,7-f][1,10]phenanthroline-11,13(10H,12H)-dione–chloroform (1/1)