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In an attempt to hydro­thermally synthesize a phase with composition Co 2 Cu(PO 4 ) 2 ·H 2 O, we obtained the title compound, Co 2.39 Cu 0.61 (PO 4 ) 2 ·H 2 O instead. Chemical analysis confirmed the presence of copper in the crystal. The crystal structure of the title compound can be described as a three- dimensional network constructed from the stacking of two types of layers extending parallel to (010). These layers are made up from more or less deformed polyhedra: CoO 6  octa­hedra, (Cu/Co)O 5  square pyramids and PO 4  tetra­hedra. The first layer is formed by pairs of edge-sharing (Cu/Co)O 5  square pyramids linked  via  a common edge of each end of the (Cu/Co) 2 O 8  dimer to PO 4  tetra­hedra. The second layer is undulating and is built up from edge-sharing CoO 6  octa­hedra. The linkage between the two layers is accomplished by PO 4  tetra­hedra. The presence of water mol­ecules in the CoO 4 (H 2 O) 2  octa­hedron also contributes to the cohesion of the layers through O—H⋯O hydrogen bonding.

Dicobalt copper bis[orthophosphate(V)] monohydrate, Co2.39Cu0.61(PO4)2·H2O

Dicobalt copper bis[orthophosphate(V)] monohydrate, Co_2.39Cu_0.61(PO₄)₂·H₂O