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Treatment of [Et 4 N] 2 [(edt) 2 Mo 2 S 2 (μ-S) 2 ] (edt = ethane­dithio­l­ate) with two equivalents of Ag(CH 3 CN) 4 ClO 4  in the presence of bis­(diphenyl­phosphino)methane (dppm) ligand gives rise to the title tetra­nuclear cluster, [Ag 2 Mo 2 (C 2 H 4 S 2 ) 2 S 4 (C 25 H 22 P 2 ) 2 ]·3C 3 H 7 NO. The complex mol­ecule and one of the dimethyl­formamide (DMF) solvent mol­ecules occupy special positions on a mirror plane. The mol­ecular structure of the complex may be visualized as being built of [Mo 2 S 2 (μ-S) 2 (edt) 2 ] 2−  dianions and [Ag 2 (dppm) 2 ] 2+  dications connected by two Ag—μ-S edt  and two Ag—μ 4 -S bonds.

acta crystallographica. section e

Bis[μ2-bis(diphenylphosphino)methane]bis(μ2-ethane-1,2-dithiolato)-μ4-sulfido-μ2-sulfido-disulfidodimolybdenum(V)disilver(I) dimethylformamide trisolvate