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The title compound, [Rh(C 10 H 7 N 2 O 2 )(C 18 H 15 P)(CO)]·(CH 3 ) 2 CO, is the second structural report of a metal complex formed with the  O , O ′-C 10 H 7 N 2 O 2  (neocupferrate) ligand. In the crystal structure, the metal centre is surrounded by one carbonyl ligand, one triphenyl­phosphine ligand and the bidentate neocupferrate ligand, forming a distorted square-planar RhCO 2 P coordination set which is best illustrated by the small O—Rh—O bite angle of 77.74 (10)°. There are no classical hydrogen-bond inter­actions observed for this complex.

Carbonyl(N-nitroso-N-oxido-1-naphtylamine-κ2O,O′)(triphenylphosphine-κP)rhodium(I) acetone solvate

Carbonyl(N-nitroso-N-oxido-1-naphtylamine-κ²O,O′)(triphenylphosphine-κP)rhodium(I) acetone solvate