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The title compound, Rb 8 [W 2 O 4 (SO 4 ) 6 ], was precipitated from a melt of tungsten(VI) oxide and rubidium sulfate in rubidium disulfate. The unit cell contains two discrete [{W VI O 2 (SO 4 ) 2 } 2 (μ-SO 4 ) 2 ] 8−  units connected by Rb–O coord­ination. The W atom is octahedrally surrounded by two oxide ligands, two terminal sulfate ligands and two bridging sulfate groups. One Rb atom is coordinated by eight O atoms, whereas the three other Rb atoms are coordinated by nine O atoms from sulfate and oxide groups, leading to distorted [RbO  x  ] polyhedra.

Octarubidium di-μ-sulfato-κ4O:O′-bis[cis-dioxido-cis-disulfatotungstate(VI)]

Octarubidium di-μ-sulfato-κ⁴O:O′-bis[cis-dioxido-cis-disulfatotungstate(VI)]