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Crystals of the title compound, NaScP 2 O 7 , were grown by a flux method. The crystal structure is isotypic with those of α-NaTiP 2 O 7 , NaYbP 2 O 7  and NaLuP 2 O 7 , and is closely related to that of NaYP 2 O 7 . The structural set-up consists of a three-dimensional framework of P 2 O 7  units that are corner-shared by ScO 6  octa­hedra, forming tunnels running parallel to [010]. The Na atoms are situated in the tunnels and are surrounded by nine O atoms in a distorted environment.

Sodium scandium diphosphate, NaScP2O7, isotypic with α-NaTi(III)P2O7

Sodium scandium diphosphate, NaScP₂O₇, isotypic with α-NaTi(III)P₂O₇